2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

Base Information

Chemical Name:2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide
CAS No.:1291079-75-8
Molecular Formula:C₃₀H₂₆N₂O₄
Molecular Weight:478.547
Hs Code.:

Synonyms:2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

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Chemical Property of 2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

Chemical Property:

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Technology Process of 2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

There total 4 articles about 2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1291079-73-6
4-(3-naphthalen-1-yl-isoxazol-5-ylmethoxy)-phenylamine

: 20143-48-0
2,6-dimethylphenoxyacetyl chloride

: 1291079-75-8
2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 40 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201001169

Reference yield:

: 1291079-78-1
3-naphthalen-1-yl-5-(4-nitro-phenoxymethyl)-isoxazole

: 1291079-75-8
2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate; zinc / methanol / 20 °C

2: triethylamine / dichloromethane / 24 h / 40 °C / Inert atmosphere

With ammonium formate; triethylamine; zinc; In methanol; dichloromethane;
DOI:10.1002/ejoc.201001169

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1291079-75-8
2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 24 h / Reflux

2: copper(ll) sulfate pentahydrate; sodium hydrogencarbonate; sodium L-ascorbate / water; tert-butyl alcohol / 3 h / 20 °C

3: ammonium formate; zinc / methanol / 20 °C

4: triethylamine / dichloromethane / 24 h / 40 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; ammonium formate; sodium hydrogencarbonate; potassium carbonate; sodium L-ascorbate; triethylamine; zinc; In methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1002/ejoc.201001169