N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

Base Information

Chemical Name:N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide
CAS No.:1291079-79-2
Molecular Formula:C₃₀H₂₈N₂O₄
Molecular Weight:480.563
Hs Code.:

Synonyms:N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

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Chemical Property of N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

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Technology Process of N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

There total 5 articles about N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1291079-75-8
2-(2,6-dimethylphenoxy)-N-(4-{[3-(naphthalen-1-yl)isoxazol-5-yl]methoxy}phenyl)acetamide

: 1291079-79-2
N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

Guidance literature:: With water; molybdenum hexacarbonyl; In acetonitrile; for 2h; Reflux;
DOI:10.1002/ejoc.201001169

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1291079-79-2
N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 24 h / Reflux

2: copper(ll) sulfate pentahydrate; sodium hydrogencarbonate; sodium L-ascorbate / water; tert-butyl alcohol / 3 h / 20 °C

3: ammonium formate; zinc / methanol / 20 °C

4: triethylamine / dichloromethane / 24 h / 40 °C / Inert atmosphere

5: water; molybdenum hexacarbonyl / acetonitrile / 2 h / Reflux

With copper(ll) sulfate pentahydrate; water; ammonium formate; sodium hydrogencarbonate; potassium carbonate; sodium L-ascorbate; triethylamine; zinc; molybdenum hexacarbonyl; In methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1002/ejoc.201001169

Reference yield:

: 1291079-78-1
3-naphthalen-1-yl-5-(4-nitro-phenoxymethyl)-isoxazole

: 1291079-79-2
N-{4-[4-amino-4-(naphthalen-1-yl)-2-oxobut-3-enyloxy]phenyl}-2-(2,6-dimethylphenoxy)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium formate; zinc / methanol / 20 °C

2: triethylamine / dichloromethane / 24 h / 40 °C / Inert atmosphere

3: water; molybdenum hexacarbonyl / acetonitrile / 2 h / Reflux

With water; ammonium formate; triethylamine; zinc; molybdenum hexacarbonyl; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201001169