(3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

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Chemical Name:(3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol
CAS No.:1015445-46-1
Molecular Formula:C₂₀H₂₃NO₄S
Molecular Weight:373.473
Hs Code.:

Synonyms:(3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

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Chemical Property of (3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

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Technology Process of (3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

There total 4 articles about (3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 2,2′-bis(diphenylphosphanyl)-5,5′-6,6′-7,7′,8,8′-octahydro-1,1′-binaphthyl

: 420132-18-9
N-(buta-2,3-dien-1-yl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

: 1015445-22-3
(3S,4S)-1-[(4-methylphenyl)sulfonyl]-4-(1-phenylethenyl)-3-pyrrolidinol

: (3R,4R)-1-[(4-methylphenyl)sulfonyl]-4-(1-phenylethenyl)-3-pyrrolidinol

: 1015445-18-7
(3S,4S)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

: 1015445-46-1
(3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

Guidance literature:: With palladium diacetate; In acetonitrile; at 20 ℃; for 24h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ol702966j

Reference yield: 74.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 76144-87-1,76189-55-4,76189-56-5,98327-87-8,136655-44-2
(S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine)

: 420132-18-9
N-(buta-2,3-dien-1-yl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

: 1015445-22-3
(3S,4S)-1-[(4-methylphenyl)sulfonyl]-4-(1-phenylethenyl)-3-pyrrolidinol

: 1015445-18-7
(3S,4S)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

: 1015445-46-1
(3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

Guidance literature:: With palladium diacetate; In acetonitrile; at 20 ℃; for 10h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ol702966j

Reference yield: 40.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 420132-18-9
N-(buta-2,3-dien-1-yl)-4-methyl-N-(2-oxoethyl)benzenesulfonamide

: 1015445-18-7
(3S,4S)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

: 1015445-46-1
(3R,4R)-4-[1-(4-methoxyphenyl)ethenyl]-1-[(4-methylphenyl)sulfonyl]-3-pyrrolidinol

Guidance literature:: With palladium diacetate; (S(P),S(P))-1,2-bis[(o-anisyl)(phenyl)phosphino]ethane; In acetonitrile; at 20 ℃; for 1h; optical yield given as %ee; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ol702966j