[N(o-C₆H₄PPh₂)2]NiCl

Base Information

Chemical Name:[N(o-C₆H₄PPh₂)2]NiCl
CAS No.:579490-55-4
Molecular Formula:C₃₆H₂₈ClNNiP₂
Molecular Weight:630.716
Hs Code.:

[N(o-C<sub>6</sub>H<sub>4</sub>PPh<sub>2</sub>)2]NiCl

Synonyms:[N(o-C₆H₄PPh₂)2]NiCl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [N(o-C₆H₄PPh₂)2]NiCl

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Technology Process of [N(o-C₆H₄PPh₂)2]NiCl

There total 6 articles about [N(o-C₆H₄PPh₂)2]NiCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: 579490-52-1
[bis(2-diphenylphosphinophenyl)amide]Li(THF)2

: 579490-55-4
chloro[bis(2-diphenylphosphinophenyl)amide]nickel(II)

Guidance literature:: In tetrahydrofuran; Li compd. reacted with Ni complex in THF at -35°C;
DOI:10.1021/om030237e

Reference yield: 93.6%

: 579490-52-1
[N(o-C₆H₄PPh₂)2]Li(THF)2

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: 579490-55-4
chloro[bis(2-diphenylphosphinophenyl)amide]nickel(II)

Guidance literature:: In tetrahydrofuran; under N2 atm. to suspn. Ni complex in THF at -35°C soln. (Ph-PNP)Li(THF)2 in THF was added dropwise and stirred at room temp. for 2 h; volatiles were removed in vacuo, residue was extd. with CH2Cl2, filteredthrough Celite and evapd. to dryness; elem. anal.;
DOI:10.1021/om050943a