1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

Base Information

Chemical Name:1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one
CAS No.:160154-72-3
Molecular Formula:C₄₇H₄₃IO₉
Molecular Weight:878.758
Hs Code.:

Synonyms:1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

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Chemical Property of 1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

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Technology Process of 1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

There total 4 articles about 1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67-56-1
methanol

: Acetic acid 3,5-bis-benzyloxy-2-[(E)-3-(2,4-bis-benzyloxy-phenyl)-acryloyl]-6-iodo-phenyl ester

: 160154-72-3
1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

Guidance literature:: With thallium(III) nitrate; In chloroform; at 40 ℃; for 2h;
DOI:10.1246/cl.1994.2101

Reference yield:

: 160154-81-4
4',6'-bis(benzyloxy)-3'-iodo-2'-(methoxymethoxy)acetophenone

: 160154-72-3
1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / ethanol / 85 °C

2: hydrochloric acid

3: pyridine

4: thallium(III) nitrate trihydrate / CHCl₃ / 2 h / 40 °C

With hydrogenchloride; potassium hydroxide; thallium(III) nitrate trihydrate; In pyridine; ethanol; chloroform;
DOI:10.1016/S0040-4039(01)01234-5

Reference yield:

: 160154-70-1
2,4,4',6'-tetrakis(benzyloxy)-2'-hydroxy-3'-iodochalcone

: 160154-72-3
1-<2-acetoxy-4,6-bis(benzyloxy)-3-iodophenyl>-2-<2,4-bis(benzyloxy)phenyl>-3,3-dimethoxypropan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: thallium(III) nitrate trihydrate / CHCl₃ / 2 h / 40 °C

With thallium(III) nitrate trihydrate; In pyridine; chloroform;
DOI:10.1016/S0040-4039(01)01234-5