2-[2-(2-Bromophenyl)-propoxy]-tetrahydropyran

Base Information

Chemical Name:2-[2-(2-Bromophenyl)-propoxy]-tetrahydropyran
CAS No.:1335095-09-4
Molecular Formula:C₁₄H₁₉BrO₂
Molecular Weight:299.208
Hs Code.:
DSSTox Substance ID:DTXSID201245186

Synonyms:1335095-09-4;2-[2-(2-bromophenyl)-propoxy]-tetrahydropyran;2-[2-(2-Bromophenyl)propoxy]tetrahydro-2H-pyran;SCHEMBL2402808;DTXSID201245186;DB-216856

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Chemical Property of 2-[2-(2-Bromophenyl)-propoxy]-tetrahydropyran

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:298.05684
Heavy Atom Count:17
Complexity:222

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(COC1CCCCO1)C2=CC=CC=C2Br

Technology Process of 2-[2-(2-Bromophenyl)-propoxy]-tetrahydropyran

There total 4 articles about 2-[2-(2-Bromophenyl)-propoxy]-tetrahydropyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 34868-16-1
2-(2-bromophenyl)propan-1-ol

: 1335095-09-4
2-[2-(2-bromophenyl)-propoxy]-tetrahydropyran

Guidance literature:: 2-(2-bromophenyl)propan-1-ol; With camphor-10-sulfonic acid; In dichloromethane; for 0.166667h; Inert atmosphere;

3,4-dihydro-2H-pyran; In dichloromethane;

Reference yield:

: 115615-34-4
(±)-methyl 2-(2-bromophenyl)propanoate

: 1335095-09-4
2-[2-(2-bromophenyl)-propoxy]-tetrahydropyran

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: camphor-10-sulfonic acid / dichloromethane / 0.17 h / Inert atmosphere

With lithium aluminium tetrahydride; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 57486-69-8
methyl 2-(2-bromophenyl)acetate

: 1335095-09-4
2-[2-(2-bromophenyl)-propoxy]-tetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.1: camphor-10-sulfonic acid / dichloromethane / 0.17 h / Inert atmosphere

With lithium aluminium tetrahydride; camphor-10-sulfonic acid; potassium tert-butylate; In tetrahydrofuran; dichloromethane;