N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide

Base Information

Chemical Name:N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide
CAS No.:80120-40-7
Molecular Formula:C₁₃H₁₇NO₂
Molecular Weight:219.283
Hs Code.:
DSSTox Substance ID:DTXSID001267607
Nikkaji Number:J1.539.044A

Synonyms:N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide;DTXSID001267607;80120-40-7

Suppliers and Price of N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:219.125928785
Heavy Atom Count:16
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)C(=O)C(=O)C1=CC=C(C=C1)C

Technology Process of N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide

There total 13 articles about N,N-Diethyl-4-methyl-alpha-oxobenzeneacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 201230-82-2
carbon monoxide

: 624-31-7
4-tolyl iodide

: 109-89-7
diethylamine

: 2728-05-4
N,N-Diethyl-p-toluamid

: 80120-40-7
N,N-diethyl-4-methyl-α-oxo-benzeneacetamide

Guidance literature:: With [bmim]PF₆; triethylamine; Pd carbene; at 80 ℃; for 0.566667h; under 15200 Torr;
DOI:10.1039/b600970k

Reference yield: 82.0%

: 201230-82-2
carbon monoxide

: 4,4'-dimethyldiphenyliodonium fluoroborate

: 109-89-7
diethylamine

: 80120-40-7
N,N-diethyl-4-methyl-α-oxo-benzeneacetamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 79.0%

: 201230-82-2
carbon monoxide

: 624-31-7
4-tolyl iodide

: 109-89-7
diethylamine

: 80120-40-7
N,N-diethyl-4-methyl-α-oxo-benzeneacetamide

Guidance literature:: With SingaCycle-A₁; potassium carbonate; In 1,4-dioxane; at 80 ℃; for 12h; under 30003 Torr; Autoclave;
DOI:10.1039/c4ob01878h