1,2,3,3-tetraphenylprop-2-en-1-one

Base Information

• Chemical Name: 1,2,3,3-tetraphenylprop-2-en-1-one
• CAS No.: 6333-11-5
• Molecular Formula: C27H20 O
• Molecular Weight: 360.455
• Mol file: 6333-11-5.mol

Synonyms:Acrylophenone,2,3,3-triphenyl- (7CI,8CI); 1,2,3,3-Tetraphenyl-2-propen-1-one;2,3,3-Triphenylacrylophenone; NSC 38799

Chemical Property of 1,2,3,3-tetraphenylprop-2-en-1-one

Chemical Property:

• Vapor Pressure: 5.62E-10mmHg at 25°C
• Boiling Point: 496°Cat760mmHg
• Flash Point: 214.3°C
• Density: 1.132g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,3,3-tetraphenylprop-2-en-1-one

There total 28 articles about 1,2,3,3-tetraphenylprop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3,3-dichloro-1,2-diphenylprop-2-en-1-one (40920-42-1) + phenylboronic acid (98-80-6) → 1,2,3,3-tetraphenylprop-2-en-1-one (6333-11-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; for 30h; Inert atmosphere; Reflux;

DOI:10.1002/adsc.201400348

Reference yield: 80.0%

3,3,4,5-tetraphenyl-2(3H)-furanone (6963-25-3) → 1,2,3,3-tetraphenylprop-2-en-1-one (6333-11-5)

Guidance literature:

In neat (no solvent); at 450 ℃; Product distribution; further temperature and time; further furanone derivatives;

DOI:10.1021/ja00336a010

Reference yield: 30.0%

3,3,4,5-tetraphenyl-2(3H)-furanone (6963-25-3) → 1,2,3,3-tetraphenylprop-2-en-1-one (6333-11-5) + benzoic acid (65-85-0,8013-63-6) + 4,5-dihydro-5-hydroxy-3,3,4,5-tetraphenyl-2(3H)-furanone (99765-21-6)

Guidance literature:

With potassium superoxide; 18-crown-6 ether; In benzene; for 24h;

upstream raw materials:

diethyl ether

1,2,3-triphenylpropane-1,3-dione

(E)-1,2,3,4-tetraphenylbut-2-ene-1,4-dione

(E)-2-phenylchalcone

Downstream raw materials:

1-(4-tert-butyl-phenyl)-2,3,3-triphenyl-propan-1-one

3-hydroxy-1.1.2.3-tetraphenyl-propane

pentaphenyl-allyl alcohol

1,2,3-triphenylindene