N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine

Base Information

• Chemical Name: N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine
• CAS No.: 136860-06-5
• Molecular Formula: C₂₆H₄₁N₃O₉
• Molecular Weight: 539.626
• Mol file: 136860-06-5.mol

Synonyms:N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine

Chemical Property of N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine

There total 1 articles about N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-glucopyranosyl amine (7284-37-9,50444-86-5) + tert-butoxycarbonyl-L-phenylalanyl-L-leucine (33014-68-5) → N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine (136860-06-5)

Guidance literature:

With 4-methyl-morpholine; isobutyl chloroformate; Yield given. Multistep reaction; 1) THF, -15 deg C, 2 min, 2a) THF, H₂O, -15 deg C, 10 min, 2b) RT, overnight;

DOI:10.1002/hlca.19910740505

Reference yield: 75.0%

N--L-phenylalanyl-L-leucyl>-β-D-glucopyranosylamine (136860-06-5) → N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate (136860-12-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1002/hlca.19910740505

upstream raw materials:

D-glucopyranosyl amine

tert-butoxycarbonyl-L-phenylalanyl-L-leucine

Downstream raw materials:

N-(L-phenylalanyl-L-leucyl)-β-D-glucopyranosylamine trifluoroacetate