6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

Base Information

Chemical Name:6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester
CAS No.:91202-44-7
Molecular Formula:C₂₅H₃₀O₃
Molecular Weight:378.511
Hs Code.:

Synonyms:6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

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Chemical Property of 6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

Chemical Property:

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Technology Process of 6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

There total 4 articles about 6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1821-23-4
1-cyclohex-1-enyl-4-methylbenzene

: 91202-44-7
6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) O₃; 2.) sulfuric acid / 1.) 20 min; 2.) 30 min, reflux

2: 60 percent / N-bromosuccinimide / CHCl₃ / 0.33 h / Heating; Irradiation

3: 1.) triphenylphosphine; 2.) potassium carbonate / 1.) xylene, reflux, 1 h; 2.) methylene chloride, tetrahydrofuran, reflux

With N-Bromosuccinimide; sulfuric acid; potassium carbonate; ozone; triphenylphosphine; In chloroform;
DOI:10.1021/ja00331a041

Reference yield:

: 106-38-7
para-bromotoluene

: 91202-44-7
6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) magnesium; 2.) toluenesulfonic acid / 1.) tetrahydrofuran, reflux, 2.5 h; 2.) toluene

2: 1.) O₃; 2.) sulfuric acid / 1.) 20 min; 2.) 30 min, reflux

3: 60 percent / N-bromosuccinimide / CHCl₃ / 0.33 h / Heating; Irradiation

4: 1.) triphenylphosphine; 2.) potassium carbonate / 1.) xylene, reflux, 1 h; 2.) methylene chloride, tetrahydrofuran, reflux

With N-Bromosuccinimide; sulfuric acid; o-toluenesulfonic acid; potassium carbonate; ozone; magnesium; triphenylphosphine; In chloroform;
DOI:10.1021/ja00331a041

Reference yield:

: 91202-39-0
6-oxo-6-p-tolylhexanoic acid methyl ester

: 91202-44-7
6-{4-[(E)-2-(4-Butyl-phenyl)-vinyl]-phenyl}-6-oxo-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / N-bromosuccinimide / CHCl₃ / 0.33 h / Heating; Irradiation

2: 1.) triphenylphosphine; 2.) potassium carbonate / 1.) xylene, reflux, 1 h; 2.) methylene chloride, tetrahydrofuran, reflux

With N-Bromosuccinimide; potassium carbonate; triphenylphosphine; In chloroform;
DOI:10.1021/ja00331a041