Technology Process of benzyl 2,4,4-tri-O-benzyllasallate
There total 6 articles about benzyl 2,4,4-tri-O-benzyllasallate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic anhydride;
In
toluene;
for 12h;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 35 percent / titanium tetrachloride / CH2Cl2 / -10 deg C then r.t.
2: 75 percent / 30 percent hydrogen peroxide, 40 percent sodium hydroxide / dioxane / 1 h / -10 °C
3: 56 percent / trifluoroacetic anhydride / toluene / 12 h
4: hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
5: 81 percent / potassium hydrogen carbonate / dimethylformamide / 24 h / Ambient temperature
6: 75 percent / trifluoroacetic anhydride / toluene / 12 h
With
sodium hydroxide; hydrogen; dihydrogen peroxide; titanium tetrachloride; potassium hydrogencarbonate; trifluoroacetic anhydride;
palladium on activated charcoal;
In
1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C98082
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / 30 percent hydrogen peroxide, 40 percent sodium hydroxide / dioxane / 1 h / -10 °C
2: 56 percent / trifluoroacetic anhydride / toluene / 12 h
3: hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h
4: 81 percent / potassium hydrogen carbonate / dimethylformamide / 24 h / Ambient temperature
5: 75 percent / trifluoroacetic anhydride / toluene / 12 h
With
sodium hydroxide; hydrogen; dihydrogen peroxide; potassium hydrogencarbonate; trifluoroacetic anhydride;
palladium on activated charcoal;
In
1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C98082
