benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Base Information

Chemical Name:benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate
CAS No.:219700-79-5
Molecular Formula:C₃₀H₂₆O₈
Molecular Weight:514.532
Hs Code.:

Synonyms:benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Suppliers and Price of benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

There total 5 articles about benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 100-39-0
benzyl bromide

: 219700-78-4
3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

: 219700-79-5
benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Guidance literature:: With potassium hydrogencarbonate; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1071/C98082

Reference yield:

: 214483-47-3
benzyl 4-benzyloxy-2-hydroxy-6-methylbenzoate

: 219700-79-5
benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 35 percent / titanium tetrachloride / CH₂Cl₂ / -10 deg C then r.t.

2: 75 percent / 30 percent hydrogen peroxide, 40 percent sodium hydroxide / dioxane / 1 h / -10 °C

3: 56 percent / trifluoroacetic anhydride / toluene / 12 h

4: hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h

5: 81 percent / potassium hydrogen carbonate / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; hydrogen; dihydrogen peroxide; titanium tetrachloride; potassium hydrogencarbonate; trifluoroacetic anhydride; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C98082

Reference yield:

: 219700-94-4
benzyl 4-benzyloxy-3-formyl-2-hydroxy-6-methylbenzoate

: 219700-79-5
benzyl 4-benzyloxy-3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / 30 percent hydrogen peroxide, 40 percent sodium hydroxide / dioxane / 1 h / -10 °C

2: 56 percent / trifluoroacetic anhydride / toluene / 12 h

3: hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h

4: 81 percent / potassium hydrogen carbonate / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; hydrogen; dihydrogen peroxide; potassium hydrogencarbonate; trifluoroacetic anhydride; palladium on activated charcoal; In 1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C98082