3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

Base Information

Chemical Name:3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid
CAS No.:219700-78-4
Molecular Formula:C₁₆H₁₄O₈
Molecular Weight:334.282
Hs Code.:

Synonyms:3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

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Chemical Property of 3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

Chemical Property:

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Technology Process of 3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

There total 4 articles about 3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219700-77-3
benzyl 4-benzyloxy-3-(2',4'-dibenzyloxy-6'-methylbenzoyloxy)-2-hydroxy-6-methylbenzoate

: 219700-78-4
3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h;
DOI:10.1071/C98082

Reference yield:

: 214483-47-3
benzyl 4-benzyloxy-2-hydroxy-6-methylbenzoate

: 219700-78-4
3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / titanium tetrachloride / CH₂Cl₂ / -10 deg C then r.t.

2: 75 percent / 30 percent hydrogen peroxide, 40 percent sodium hydroxide / dioxane / 1 h / -10 °C

3: 56 percent / trifluoroacetic anhydride / toluene / 12 h

4: hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h

With sodium hydroxide; hydrogen; dihydrogen peroxide; titanium tetrachloride; trifluoroacetic anhydride; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; ethyl acetate; toluene;
DOI:10.1071/C98082

Reference yield:

: 219700-94-4
benzyl 4-benzyloxy-3-formyl-2-hydroxy-6-methylbenzoate

: 219700-78-4
3-(2',4'-dihydroxy-6'-methylbenzoyloxy)-2,4-dihydroxy-6-methylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 30 percent hydrogen peroxide, 40 percent sodium hydroxide / dioxane / 1 h / -10 °C

2: 56 percent / trifluoroacetic anhydride / toluene / 12 h

3: hydrogen / 10 percent palladium on carbon / ethyl acetate / 16 h

With sodium hydroxide; hydrogen; dihydrogen peroxide; trifluoroacetic anhydride; palladium on activated charcoal; In 1,4-dioxane; ethyl acetate; toluene;
DOI:10.1071/C98082