C₉H₁₀N₂O₄*ClH

Base Information

• Chemical Name: C₉H₁₀N₂O₄*ClH
• CAS No.: 195070-55-4
• Molecular Formula: C₉H₁₀N₂O₄*ClH
• Molecular Weight: 246.65
• Mol file: 195070-55-4.mol

Synonyms:C₉H₁₀N₂O₄*ClH

Chemical Property of C₉H₁₀N₂O₄*ClH

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₁₀N₂O₄*ClH

There total 2 articles about C₉H₁₀N₂O₄*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + D-(-)-α-(m-nitrophenyl)glycine (4885-81-8) → C9H10N2O4*ClH (195070-55-4)

Guidance literature:

With thionyl chloride; at 0 ℃; for 6h;

DOI:10.1016/j.tet.2011.07.047

Reference yield:

(R)-phenylglycine (875-74-1) → C9H10N2O4*ClH (195070-55-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid / water / 3 h / 0 °C

2: thionyl chloride / 6 h / 0 °C

With thionyl chloride; sulfuric acid; nitric acid; In water;

DOI:10.1016/j.tet.2011.07.047

Reference yield:

C9H10N2O4*ClH (195070-55-4) → D-(-)-α-(m-nitrophenyl)glycine hydrazide (1337535-15-5)

Guidance literature:

With hydrazine hydrate; In methanol; for 24h;

DOI:10.1016/j.tet.2011.07.047

upstream raw materials:

methanol

D-(-)-α-(m-nitrophenyl)glycine

(R)-phenylglycine

Downstream raw materials:

D-(-)-α-(m-nitrophenyl)glycine hydrazide

5-(m-nitrophenyl)-3-phenyl-4,5-dihydro-1,2,4-triazin-6(1H)-one