(S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

Base Information

Chemical Name:(S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine
CAS No.:1464832-63-0
Molecular Formula:C₁₇H₁₆ClN₃O₂S
Molecular Weight:361.852
Hs Code.:

Synonyms:(S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

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Chemical Property of (S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

Chemical Property:

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Technology Process of (S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

There total 10 articles about (S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1464832-62-9
2-((1S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethyl)-isoindoline-1,3-dione

: 1464832-63-0
(S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

Guidance literature:: With hydrazine; In water; at 65 ℃; for 6h; Inert atmosphere;

Reference yield:

: 1464832-59-4
(S)-2-(1-(3,5-dichloroquinoxalin-2-yl)ethyl)isoindoline-1,3-dione

: 1464832-63-0
(S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 4 h / 100 °C / Inert atmosphere

2: Oxone / water; dichloromethane / 96 h / 15 - 21 °C

3: hydrazine / water / 6 h / 65 °C / Inert atmosphere

With Oxone; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; hydrazine; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1464832-61-8
2-((1S)-1-(5-chloro-3-(2-(methylthio)phenyl)quinoxalin-2-yl)ethyl)isoindoline-1,3-dione

: 1464832-63-0
(S)-1-(5-chloro-3-(2-(methylsulfonyl)phenyl)quinoxalin-2-yl)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / water; dichloromethane / 96 h / 15 - 21 °C

2: hydrazine / water / 6 h / 65 °C / Inert atmosphere

With Oxone; hydrazine; In dichloromethane; water;