2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

Base Information

Chemical Name:2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole
CAS No.:163273-59-4
Molecular Formula:C₅₂H₉₃GeNOSeSi₆
Molecular Weight:1068.38
Hs Code.:

Synonyms:2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

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Chemical Property of 2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

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Technology Process of 2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

There total 7 articles about 2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 163273-57-2
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germaneselone

: 2904-57-6
mesitylenecarbonitrile oxide

: 163273-59-4
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

Guidance literature:: In hexane; react. of the components in hexane in a closed ampoule at 100°C;

Reference yield: 90.0%

: 163273-58-3
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4,5-dimethyl-1-selena-2-germacyclohex-4-ene

: 2904-57-6
mesitylenecarbonitrile oxide

: 163273-59-4
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

Guidance literature:: In hexane; freezing, evacuation, sealing, heating (50°C, 2h); chromatography (SiO2, hexane/CH2Cl2 (5:1));
DOI:10.1021/ja991147x

Reference yield:

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

: 163273-59-4
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-triisopropylphenyl)-4-mesityl-1,3,5,2-oxaselenazagermole

Guidance literature:: Multi-step reaction with 4 steps

1: LiC₁₀H₈ / tetrahydrofuran

2: tetrahydrofuran

3: hexane

With LiC₁₀H₈; In tetrahydrofuran; hexane;
DOI:10.1021/ja991147x