2-phenylallyl methanesulfonate

Base Information

Chemical Name:2-phenylallyl methanesulfonate
CAS No.:1204186-01-5
Molecular Formula:C₁₀H₁₂O₃S
Molecular Weight:212.269
Hs Code.:

Synonyms:2-phenylallyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenylallyl methanesulfonate

Chemical Property:

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Technology Process of 2-phenylallyl methanesulfonate

There total 3 articles about 2-phenylallyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 6006-81-1
3-hydroxy-2-phenylpropene

: 7143-01-3
Methanesulfonic anhydride

: 1204186-01-5
2-phenylallyl methanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 25 ℃;
DOI:10.3390/MOLECULES25102463

Reference yield:

: 6006-81-1
3-hydroxy-2-phenylpropene

: 124-63-0
methanesulfonyl chloride

: 1204186-01-5
2-phenylallyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1204186-01-5
2-phenylallyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / diethyl ether / 1.5 h / Inert atmosphere; Reflux; Sealed tube

1.2: 0.5 h / 20 °C / Inert atmosphere; Sealed tube

1.3: 24 h / Inert atmosphere; Reflux; Sealed tube

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere; Sealed tube

With iodine; magnesium; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1002/anie.201803277