Technology Process of C72H64O17
There total 7 articles about C72H64O17 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(E)-3-(4-methoxyphenyl)acrylic acid;
With
triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate;
In
dichloromethane;
at 20 ℃;
for 0.5h;
C22H24O7;
With
dmap;
In
dichloromethane;
at 20 ℃;
DOI:10.1007/s11745-010-3482-4
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water / pH 3 - 4.4
2.1: hydrogenchloride / water
3.1: Raney Ni / 1,4-dioxane / 1 h / 80 °C
4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate / dichloromethane / 0.5 h / 20 °C
4.2: 20 °C
5.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate / dichloromethane / 0.5 h / 20 °C
5.2: 20 °C
With
hydrogenchloride; water; triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1007/s11745-010-3482-4
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: acetic acid / water / 20 °C / pH 7.2
1.2: 1.5 h / pH 7.2 - 7.5
2.1: 5% Pd-BaSO4; hydrogen; acetic acid / water / 15 h / 20 °C / pH 4.2
3.1: water / pH 3 - 4.4
4.1: hydrogenchloride / water
5.1: Raney Ni / 1,4-dioxane / 1 h / 80 °C
6.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate / dichloromethane / 0.5 h / 20 °C
6.2: 20 °C
7.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate / dichloromethane / 0.5 h / 20 °C
7.2: 20 °C
With
hydrogenchloride; 5% Pd-BaSO4; water; hydrogen; acetic acid; triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1007/s11745-010-3482-4