4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

Base Information

Chemical Name:4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol
CAS No.:1356339-53-1
Molecular Formula:C₂₆H₃₃BrN₄O₃
Molecular Weight:529.477
Hs Code.:

Synonyms:4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

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Chemical Property of 4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

Chemical Property:

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Technology Process of 4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

There total 5 articles about 4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 62402-19-1
N-(2-methoxyethyl)-N-(pyridin-2-ylmethyl)amine

: 72109-66-1
2,6-bis(bromomethyl)-4-bromophenol

: 1356339-53-1
4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c1dt11187f

Reference yield:

: 150975-29-4
2-methoxy-N-((pyridin-2-yl)methylene)ethanamine

: 1356339-53-1
4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 °C

2: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1dt11187f

Reference yield:

: 106-41-2
4-bromo-phenol

: 1356339-53-1
4-bromo-2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 288 h / 20 °C

2: hydrogen bromide / acetic acid / 0.17 h

3: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C

With hydrogen bromide; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid;
DOI:10.1039/c1dt11187f