N-methylallylaminophenylvinylborane

Base Information

Chemical Name:N-methylallylaminophenylvinylborane
CAS No.:287735-73-3
Molecular Formula:C₁₂H₁₆BN
Molecular Weight:185.077
Hs Code.:

Synonyms:N-methylallylaminophenylvinylborane

Suppliers and Price of N-methylallylaminophenylvinylborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methylallylaminophenylvinylborane

Chemical Property:

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Technology Process of N-methylallylaminophenylvinylborane

There total 1 articles about N-methylallylaminophenylvinylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 627-37-2
N-methyl-N-allylamine

: 287735-76-6
phenyl vinyl boron chloride

: 287735-73-3
N-methylallylaminophenylvinylborane

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 3h;
DOI:10.1021/ol0001113

Reference yield: 86.0%

: 287735-73-3
N-methylallylaminophenylvinylborane

: 287735-74-4
1,5-dihydro-1-methyl-2-phenyl-1,2-azaborole

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 25 ℃; for 10h;
DOI:10.1021/ol0001113

Reference yield:

: 287735-73-3
N-methylallylaminophenylvinylborane

: 2,3-dihydro-1-methyl-2-phenyl-1H-1,2-azaborol-3-yllithium

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / (Cy₃P)2(PhCH)RuCl₂ / CH₂Cl₂ / 10 h / 25 °C

2: 81 percent / LDA / diethyl ether / 5 h / -78 - 25 °C

With Grubbs catalyst first generation; lithium diisopropyl amide; In diethyl ether; dichloromethane; 1: Cyclization / 2: deprotonation;
DOI:10.1021/ol0001113