2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

Base Information

Chemical Name:2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile
CAS No.:934177-24-9
Molecular Formula:C₁₇H₁₄N₄O₄
Molecular Weight:338.323
Hs Code.:

Synonyms:2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

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Chemical Property of 2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

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Technology Process of 2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

There total 3 articles about 2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: (S)-3-(3-nitrobenzylidene)amino-4-phenyloxazolidin-2-one

: 7677-24-9
trimethylsilyl cyanide

: 934177-24-9
2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

: 934177-32-9
(O₂NC₆H₄)CH(CN)NHC₃H₃NO₂C₆H₅

Guidance literature:: With In(OSO₂CF₃)3; In dichloromethane; for 48h;
DOI:10.3987/com-06-s(w)3

Reference yield:

: 99395-88-7,7480-32-2
(S)-4-phenyl-2-oxazolidinone

: 934177-24-9
2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dioxane

2: 89 percent / MgSO₄; p-TsOH / toluene / 0.17 h / Heating

3: 53 percent / In(OTf)3 / CH₂Cl₂ / 48 h

With In(OSO₂CF₃)3; sodium hydride; magnesium sulfate; toluene-4-sulfonic acid; In 1,4-dioxane; dichloromethane; toluene; 3: Strecker reaction;
DOI:10.3987/com-06-s(w)3

Reference yield:

: 458524-24-8
N-amino S-(+)-4-phenyl-2-oxazolidinone

: 934177-24-9
2-(3-nitrophenyl)-2-[(S)-(2-oxo-4-phenyloxazolidin-3-yl)amino]acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / MgSO₄; p-TsOH / toluene / 0.17 h / Heating

2: 53 percent / In(OTf)3 / CH₂Cl₂ / 48 h

With In(OSO₂CF₃)3; magnesium sulfate; toluene-4-sulfonic acid; In dichloromethane; toluene; 2: Strecker reaction;
DOI:10.3987/com-06-s(w)3