(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Base Information

Chemical Name:(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate
CAS No.:1357485-73-4
Molecular Formula:C₅₂H₆₂N₂O₉Si
Molecular Weight:887.158
Hs Code.:

(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Synonyms:(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Suppliers and Price of (2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

There total 5 articles about (2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1357485-72-3
(2S,3S)-2-amino-4-(benzyloxy)-3-(tertbutyldimethylsilyloxy)-4-oxobutanoic acid

: 172611-73-3
4-{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutyl]amino}benzyl alcohol

: 1357485-73-4
(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1007/s00726-010-0806-x

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1357485-73-4
(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; acetone / 2 h

2: dmap; diisopropyl-carbodiimide / dichloromethane

With dmap; sodium hydrogencarbonate; diisopropyl-carbodiimide; In dichloromethane; water; acetone;
DOI:10.1007/s00726-010-0806-x

Reference yield:

: 1357485-71-2
(2S,3S)-2-amino-4-(benzyloxy)-3-(tertbutyldimethylsilyloxy)-4-oxobutanoic acid

: 1357485-73-4
(2S,3S)-1-(4-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)benzyl) 4-benzyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tertbutyldimethylsilyloxy)succinate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; acetone / 2 h

2: dmap; diisopropyl-carbodiimide / dichloromethane

With dmap; sodium hydrogencarbonate; diisopropyl-carbodiimide; In dichloromethane; water; acetone;
DOI:10.1007/s00726-010-0806-x