C₁₂H₁₅F₂NO₃

Base Information

Chemical Name:C₁₂H₁₅F₂NO₃
CAS No.:1445796-42-8
Molecular Formula:C₁₂H₁₅F₂NO₃
Molecular Weight:259.253
Hs Code.:

C<sub>12</sub>H<sub>15</sub>F<sub>2</sub>NO<sub>3</sub>

Synonyms:C₁₂H₁₅F₂NO₃

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Chemical Property of C₁₂H₁₅F₂NO₃

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Technology Process of C₁₂H₁₅F₂NO₃

There total 5 articles about C₁₂H₁₅F₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1445796-41-7
C₁₄H₁₇F₂NO₄

: 1445796-42-8
C₁₂H₁₅F₂NO₃

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 2646-91-5
2,3-difluorobenzaldehyde

: 1445796-42-8
C₁₂H₁₅F₂NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; sulfuric acid / 4 h / 60 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 2.5 h / 0 - 20 °C

3: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

4: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane / 100 °C

5: sodium tetrahydroborate / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; sulfuric acid; caesium carbonate; triethylamine; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol;

Reference yield:

: 887585-71-9
(5-bromo-2,3-difluorophenyl)methanol

: 1445796-42-8
C₁₂H₁₅F₂NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

2: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane / 100 °C

3: sodium tetrahydroborate / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; triethylamine; XPhos; In tetrahydrofuran; 1,4-dioxane;