C₄₉H₇₂O₁₂S₆

Base Information

• Chemical Name: C₄₉H₇₂O₁₂S₆
• CAS No.: 1636900-06-5
• Molecular Formula: C₄₉H₇₂O₁₂S₆
• Molecular Weight: 1045.5
• Mol file: 1636900-06-5.mol

Synonyms:C₄₉H₇₂O₁₂S₆

Chemical Property of C₄₉H₇₂O₁₂S₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₉H₇₂O₁₂S₆

There total 2 articles about C₄₉H₇₂O₁₂S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

5,5’-(propane-2,2-diyl)bis(2-allyloxy-1,3-bis(allyloxymethyl)benzene) (1636900-03-2) + tiolacetic acid (507-09-5) → C49H72O12S6 (1636900-06-5)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; at 20 - 65 ℃; for 16.5h; Inert atmosphere;

DOI:10.3762/bjoc.10.180

Reference yield:

5,5'-isopropylidenebis(metaxylene-2,α,α'-triol) (3957-22-0) → C49H72O12S6 (1636900-06-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 48 h / 20 °C / Inert atmosphere

2.1: 2,2'-azobis(isobutyronitrile) / tetrahydrofuran / 16.5 h / 20 - 65 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;

DOI:10.3762/bjoc.10.180

Reference yield: 45.0%

C49H72O12S6 (1636900-06-5) → C37H60O6S6 (1636900-08-7)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; methanol; at 60 ℃; for 24h; Inert atmosphere;

DOI:10.3762/bjoc.10.180

upstream raw materials:

5,5'-isopropylidenebis(metaxylene-2,α,α'-triol)

5,5’-(propane-2,2-diyl)bis(2-allyloxy-1,3-bis(allyloxymethyl)benzene)

tiolacetic acid

Downstream raw materials:

C₃₇H₆₀O₆S₆