diphenylphosphine

Base Information

Chemical Name:diphenylphosphine
CAS No.:74492-07-2
Molecular Formula:C₂₃H₂₆NP
Molecular Weight:347.44
Hs Code.:

<S-2-(dimethylamino)-3-phenylpropyl>diphenylphosphine

Synonyms:diphenylphosphine

Suppliers and Price of diphenylphosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenylphosphine

Chemical Property:

Purity/Quality:

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Technology Process of diphenylphosphine

There total 8 articles about diphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 74492-03-8
(S)-(+)-2-N,N-dimethylamino-3-phenyl-1-propylchloride hydrochloride

: 603-35-0
triphenylphosphine

: 74492-07-2
diphenylphosphine

Guidance literature:: With ammonia; sodium; at -78 ℃; for 12h;
DOI:10.1039/b003514i

Reference yield: 47.0%

: 74492-03-8
(S)-(+)-2-N,N-dimethylamino-3-phenyl-1-propylchloride hydrochloride

: 829-85-6
diphenylphosphane

: 74492-07-2
diphenylphosphine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jo00161a013

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 74492-07-2
diphenylphosphine

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / Pd-C

2: lithium aluminum hydride / tetrahydrofuran

3: hydrogen chloride, thionyl chloride / CHCl₃

4: potassium tert-butoxide / tetrahydrofuran

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; potassium tert-butylate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; chloroform;
DOI:10.1016/S0040-4039(00)93629-3