1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

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Chemical Name:1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone
CAS No.:1315306-89-8
Molecular Formula:C₂₇H₂₇NO₃S
Molecular Weight:445.582
Hs Code.:

Synonyms:1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

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Chemical Property of 1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

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Technology Process of 1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

There total 4 articles about 1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911028-87-0
(2R,3R)-2-phenyl-3-[(E)-2-phenyl-1-ethenyl]-1-tosylaziridine

: 78-94-4,25038-87-3
methyl vinyl ketone

: 1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

: 1315306-89-8
1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

Guidance literature:: methyl vinyl ketone; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾-chloroform; tetrabutyl-ammonium chloride; tris-(o-tolyl)phosphine; In tert-butyl methyl ether; pentane; at 20 ℃; for 0.333333h;

(2R,3R)-2-phenyl-3-[(E)-2-phenyl-1-ethenyl]-1-tosylaziridine; In tert-butyl methyl ether; pentane; at 20 ℃; for 24h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201101389

Reference yield:

: 1269141-77-6
(1R,4R,5R,6R)-6-benzyl-4,7,7-trimethyl-6-thiabicyclo[3.2.1]octan-6-ium trifluoromethanesulfonate

: 1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

: 1315306-89-8
1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0 - 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾-chloroform; tetrabutyl-ammonium chloride; tris-(o-tolyl)phosphine / tert-butyl methyl ether; pentane / 0.33 h / 20 °C

2.2: 24 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾-chloroform; tetrabutyl-ammonium chloride; potassium carbonate; tris-(o-tolyl)phosphine; In tert-butyl methyl ether; acetonitrile; pentane;
DOI:10.1002/anie.201101389

Reference yield:

: 137845-37-5,144381-72-6,51985-30-9
4-methyl-N-(3-phenylallylidene)benzenesulfonamide

: 1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

: 1315306-89-8
1-(1-[(4-methylphenyl)sulfonyl]-5-phenyl-4-[(E)-2-phenylethen-1-yl]tetrahydro-1H-pyrrol-3-yl)-1-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0 - 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾-chloroform; tetrabutyl-ammonium chloride; tris-(o-tolyl)phosphine / tert-butyl methyl ether; pentane / 0.33 h / 20 °C

2.2: 24 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾-chloroform; tetrabutyl-ammonium chloride; potassium carbonate; tris-(o-tolyl)phosphine; In tert-butyl methyl ether; acetonitrile; pentane;
DOI:10.1002/anie.201101389