Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

Base Information

Chemical Name:Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp
CAS No.:257884-83-6
Molecular Formula:C₅₁H₄₀P₂Ru
Molecular Weight:815.896
Hs Code.:

Ru(C<sub>.</sub>tplbond.CC<sub>6</sub>H<sub>4</sub>C<sub>.</sub>tplbond.CH)(PPh<sub>3</sub>)2Cp

Synonyms:Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

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Chemical Property of Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

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Technology Process of Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

There total 1 articles about Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67-56-1
methanol

: 256391-99-8
Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

: 257884-83-6
Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

Guidance literature:: With Bu₄NF; In tetrahydrofuran; methanol; N2-atmosphere; stirring in THF/MeOH=4:1 v/v overnight; solvent removal (reduced pressure), chromy. (Al2O3, Me2CO/hexane=3:7), evapn.; elem. anal.;
DOI:10.1016/S0022-328X(99)00487-8

Reference yield: 90.0%

: tricarbonylcyclopentadienyltungsten(II) chloride

: 257884-83-6
Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

: (Cp(OC)3W)(μ-C.tplbond.CC6H4C.tplbond.C)(Ru(PPh3)2Cp)

Guidance literature:: With Et₂NH; copper(l) iodide; In diethylamine; N2-atmosphere; stirring in dark for 1 h; collection, washing (hexane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(99)00487-8

Reference yield: 85.0%

: hexafluorophosphoric acid

: 257884-83-6
Ru(C_.tplbond.CC₆H₄C_.tplbond.CH)(PPh₃)2Cp

: 257884-89-2
[Ru(=C=CHC₆H₄C_.tplbond.CH)(PPh₃)2Cp][PF₆]

Guidance literature:: In methanol; N2-atmosphere; stirring at room temp. for 10 min; solvent removal, dissoln. in CH2Cl2, addn. to stirred Et2O (pptn.); elem. anal.;
DOI:10.1016/S0022-328X(99)00487-8