benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Base Information

Chemical Name:benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate
CAS No.:1196967-57-3
Molecular Formula:C₄₆H₄₁N₃O₁₀S
Molecular Weight:827.912
Hs Code.:

benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Synonyms:benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

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Chemical Property of benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

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Technology Process of benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

There total 1 articles about benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1196967-89-1
benzyl (11bR)-11b-(4-amino-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1196967-57-3
benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.200902192

Reference yield: 84.0%

: 1196967-57-3
benzyl (11bR)-11b-(4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

: 1196967-59-5
C₄₆H₄₁N₃O₁₁S

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200902192