1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride

Base Information

• Chemical Name: 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride
• CAS No.: 1248589-75-4
• Molecular Formula: C₁₆H₂₄N₃*Cl
• Molecular Weight: 293.84
• Mol file: 1248589-75-4.mol

Synonyms:1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride

Chemical Property of 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride

There total 4 articles about 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride hydrochloride (1248589-76-5) → 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride (1248589-75-4)

Guidance literature:

With sodium hydroxide; In methanol; at 20 ℃; for 1h;

Reference yield:

N-benzylidene-3-(1H-imidazo-1-lyl)-1-propaneamine (820220-10-8) + 2-chloromethyl-1,3,5-trimethylbenzene (1585-16-6) → 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride (1248589-75-4)

Guidance literature:

N-benzylidene-3-(1H-imidazo-1-lyl)-1-propaneamine; 2-chloromethyl-1,3,5-trimethylbenzene; In toluene; at 100 ℃; for 5h;

In water; toluene; at 80 ℃; for 1h;

Reference yield:

3-(1H-imidazol-1-yl)propan-1-amine (5036-48-6) → 1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride (1248589-75-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

2.1: toluene / 5 h / 100 °C

2.2: 1 h / 80 °C

With toluene-4-sulfonic acid; In toluene;

upstream raw materials:

3-(1H-imidazol-1-yl)propan-1-amine

N-benzylidene-3-(1H-imidazo-1-lyl)-1-propaneamine

2-chloromethyl-1,3,5-trimethylbenzene

1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride hydrochloride

Downstream raw materials:

1-[(2,4,6-trimethylphenyl)methyl]-3-(3-aminopropyl)imidazolium chloride hydrochloride