ethyl 2-((4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)thio)acetate

Base Information

• Chemical Name: ethyl 2-((4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)thio)acetate
• CAS No.: 332909-79-2
• Molecular Formula: C₁₇H₁₆N₄O₂S
• Molecular Weight: 340.406
• Mol file: 332909-79-2.mol

Synonyms:ethyl [(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl] acetate

Chemical Property of ethyl 2-((4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)thio)acetate

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Technology Process of ethyl 2-((4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)thio)acetate

There total 2 articles about ethyl 2-((4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)thio)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

chloroacetic acid ethyl ester (105-39-5) + 4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazole-3-thiol (57600-03-0) → ethyl [(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl] acetate (332909-79-2)

Guidance literature:

With potassium carbonate; In acetone; at 20 - 60 ℃; for 11h; chemoselective reaction;

DOI:10.1134/S1070428017060203

Reference yield: 71.4%

ethyl bromoacetate (105-36-2) + 4-phenyl-3-(pyridin-3-yl)-Δ2-1,2,4-triazoline-5-thione (57600-03-0) → ethyl [(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl] acetate (332909-79-2)

Guidance literature:

With ethanol; sodium; at 20 ℃;

DOI:10.1080/10426507.2011.625511

Reference yield: 90.2%

ethyl [(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl] acetate (332909-79-2) → 2-{[4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl]sulfanyl}acetohydrazide (1359941-48-2)

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 24h;

DOI:10.1080/10426507.2011.625511

upstream raw materials:

ethyl bromoacetate

4-phenyl-3-(pyridin-3-yl)-Δ²-1,2,4-triazoline-5-thione

chloroacetic acid ethyl ester

4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazole-3-thiol

Downstream raw materials:

4-ethoxycarbonyl-1-{[(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl} thiosemicarbazide

4-(4-methoxybenzyl)-5-{[(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl]methyl}-4H-1,2,4-triazole-3(2H)-thione

4-allyl-5-{[(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl]methyl}-4H-1,2,4-triazole-3(2H)-thione

(2-aminophenyl)-5-{[(4-phenyl-5-(pyridin-3-yl)-4H-1,2,4-triazol-3-yl)sulfanyl]methyl}-1,3,4-thiadiazole

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