3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Base Information

Chemical Name:3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine
CAS No.:99896-28-3
Molecular Formula:C₄₅H₄₃NO₆
Molecular Weight:693.84
Hs Code.:

3,9-bis(benzyloxy)-2,10-dimethoxy-6-<bis(4-methoxyphenyl)methyl>-6,7-dihydro-5H-dibenz<c,e>azepine

Synonyms:3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Suppliers and Price of 3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

There total 3 articles about 3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 19293-62-0
p,p'-dimethoxybenzhydrylamine

: 99896-38-5
4,4'-bis(benzyloxy)-5,5'-dimethoxybiphenyl-2,2'-dicarbaldehyde

: 99896-28-3
3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Guidance literature:: With sodium dithionite; In methanol; water; N,N-dimethyl-formamide; 90-100 deg C, 1 h; reflux, 2 h;

Reference yield:

: 82584-00-7
3-benzyloxy-6-iodo-4-methoxybenzaldehyde

: 99896-28-3
3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / activated cooper bronze / 5 h / 200 - 220 °C

2: 90 percent / sodium dithionite / dimethylformamide; methanol; H₂O / 90-100 deg C, 1 h; reflux, 2 h

With sodium dithionite; copper bronze; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 99896-28-3
3,9-bis(benzyloxy)-2,10-dimethoxy-6--6,7-dihydro-5H-dibenzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / iodine, silver trifluoroacetate / CHCl₃ / 1 h / Ambient temperature

2: 75 percent / activated cooper bronze / 5 h / 200 - 220 °C

3: 90 percent / sodium dithionite / dimethylformamide; methanol; H₂O / 90-100 deg C, 1 h; reflux, 2 h

With sodium dithionite; copper bronze; iodine; silver trifluoroacetate; In methanol; chloroform; water; N,N-dimethyl-formamide;