2-benzyl-4-fluorobenzaldehyde

Base Information

Chemical Name:2-benzyl-4-fluorobenzaldehyde
CAS No.:1610973-44-8
Molecular Formula:C₁₄H₁₁FO
Molecular Weight:214.239
Hs Code.:

Synonyms:2-benzyl-4-fluorobenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyl-4-fluorobenzaldehyde

Chemical Property:

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Technology Process of 2-benzyl-4-fluorobenzaldehyde

There total 3 articles about 2-benzyl-4-fluorobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 591-50-4
iodobenzene

: 63082-45-1
4-fluoro-2-methylbenzaldehyde

: 1610973-44-8
2-benzyl-4-fluorobenzaldehyde

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; water; silver trifluoroacetate; hydrazine carboxamide; butyric acid; at 120 ℃; for 48h; Sealed tube;
DOI:10.1002/adsc.201901392

Reference yield:

: C₂₁H₁₈FN

: 1610973-44-8
2-benzyl-4-fluorobenzaldehyde

Guidance literature:: With hydrogenchloride; water; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201303809

Reference yield:

: 1610973-72-2
C₁₄H₁₁F₂N

: 100-39-0
benzyl bromide

: 1610973-44-8
2-benzyl-4-fluorobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; zinc / N,N-dimethyl acetamide / 3 h / 80 °C / Inert atmosphere; Schlenk technique

1.2: 24 h / 70 °C / Inert atmosphere; Schlenk technique

2.1: hydrogenchloride; water / 0.5 h / 20 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; water; iodine; zinc; In N,N-dimethyl acetamide; 1.2: |Negishi Coupling;
DOI:10.1002/chem.201303809