(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Chemical Name:(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal
CAS No.:1335130-86-3
Molecular Formula:C₄₀H₄₇N₅O₉S₂
Molecular Weight:805.973
Hs Code.:

(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Synonyms:(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Chemical Property of (2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Technology Process of (2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

There total 6 articles about (2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1037070-06-6
(2S)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-pyrrolidine-2-carboxaldehyde diethyl-dithioacetal

: 1335130-77-2
(E)-3-(4-(4-azidobutyloxy)-3-methoxyphenyl)-1-(2-hydroxyphenyl)prop-2-en-1-one

: 1335130-86-3
(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/j.ejmech.2011.05.050

Reference yield:

: 1335130-74-9
4-(4-azidobutyloxy)-3-methoxybenzaldehyde

: 1335130-86-3
(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol; water / 12 h / 20 °C

1.2: pH 1

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 12 h / 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; potassium hydroxide; In methanol; water; tert-butyl alcohol; 1.1: Aldol condensation;
DOI:10.1016/j.ejmech.2011.05.050

Reference yield:

: 1415683-28-1
3-(4-bromobutoxy)-4-methoxybenzaldehyde

: 1335130-86-3
(2S)-N-{4-{(1-(4-(4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxy phenoxy)butyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / 6 h / 80 °C

2.1: potassium hydroxide / methanol; water / 12 h / 20 °C

2.2: pH 1

3.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 12 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; potassium hydroxide; In methanol; water; tert-butyl alcohol; 2.1: Aldol condensation;
DOI:10.1016/j.ejmech.2011.05.050