C₁₁H₁₃BrO₃

Base Information

Chemical Name:C₁₁H₁₃BrO₃
CAS No.:1374020-75-3
Molecular Formula:C₁₁H₁₃BrO₃
Molecular Weight:273.126
Hs Code.:

C<sub>11</sub>H<sub>13</sub>BrO<sub>3</sub>

Synonyms:C₁₁H₁₃BrO₃

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Chemical Property of C₁₁H₁₃BrO₃

Chemical Property:

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Technology Process of C₁₁H₁₃BrO₃

There total 4 articles about C₁₁H₁₃BrO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1374020-73-1
C₁₁H₁₃BrO₂

: 1374020-75-3
C₁₁H₁₃BrO₃

Guidance literature:: With sodium chlorite; aminosulfonic acid; sodium acetate; In 1,4-dioxane; water; dimethyl sulfoxide; at 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/ja211305j

Reference yield:

: 1374020-68-4
C₉H₉BrO₂

: 1374020-75-3
C₁₁H₁₃BrO₃

Guidance literature:: Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 15 h / 100 °C / Inert atmosphere

3: sodium chlorite; aminosulfonic acid; sodium acetate / 1,4-dioxane; water; dimethyl sulfoxide / 0.75 h / 20 °C / Inert atmosphere

With sodium chlorite; aminosulfonic acid; sodium acetate; boron tribromide; potassium carbonate; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja211305j

Reference yield:

: 32723-67-4
3-methyl-4-anisaldehyde

: 1374020-75-3
C₁₁H₁₃BrO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium; N,N',N'-trimethylenediamine / tetrahydrofuran; cyclohexane / -20 °C / Inert atmosphere

1.2: 0.42 h / -78 °C / Inert atmosphere

2.1: boron tribromide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 100 °C / Inert atmosphere

4.1: sodium chlorite; aminosulfonic acid; sodium acetate / 1,4-dioxane; water; dimethyl sulfoxide / 0.75 h / 20 °C / Inert atmosphere

With sodium chlorite; n-butyllithium; aminosulfonic acid; sodium acetate; boron tribromide; potassium carbonate; N,N',N'-trimethylenediamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja211305j