1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane

Base Information

• Chemical Name: 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane
• CAS No.: 125682-99-7
• Molecular Formula: C₄₃H₅₃N₅O₁₂S₅
• Molecular Weight: 992.25

Synonyms:1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane

Chemical Property of 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane

Chemical Property:

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Technology Process of 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane

There total 3 articles about 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanesulfonyl chloride (124-63-0) + 1,11-bis<6-(hydroxymethyl)pyridin-2-yl>-2,6,10-tritosyl-2,6,10-triazaundecane (125682-98-6) → 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane (125682-99-7)

Guidance literature:

With triethylamine; In dichloromethane; for 3h; Ambient temperature;

DOI:10.1002/hlca.19890720525

Reference yield:

1,5,9-Tritosyl-1,5,9-triazanonane (35980-64-4) → 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane (125682-99-7)

Guidance literature:

Multi-step reaction with 3 steps

1: Na / 2 h / Heating

2: 50 percent / dimethylformamide / 5 h / 90 °C

3: 100 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With sodium; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

Reference yield:

N,N',N''-tritosyl-4-aza-1,7-heptandiamine disodium salt (56479-75-5) → 1,11-bis<<6-<(mesyloxy)methyl>pyridin-2-yl>methyl>-2,6,10-tritosyl-2,6,10-triazaundecane (125682-99-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 50 percent / dimethylformamide / 5 h / 90 °C

2: 100 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

upstream raw materials:

methanesulfonyl chloride

1,11-bis<6-(hydroxymethyl)pyridin-2-yl>-2,6,10-tritosyl-2,6,10-triazaundecane

1,5,9-Tritosyl-1,5,9-triazanonane

N,N',N''-tritosyl-4-aza-1,7-heptandiamine disodium salt

Downstream raw materials:

3,7,11,19,27-pentatosyl-3,7,11,19,27,33,34,35-octaazatetracyclo<27.3.1.1^13,17.1^21,25>pentatriaconta-1(33),13(34),14,16,21(35),22,24,29,31-nonaene

3,6,9,17,21,25-hexatosyl-3,6,9,17,21,25,31,32-octaazatricyclo<25.3.1.1^1,15>dotriaconta-1(31),11(32),12,14,27,29-hexaene

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