C₂₄H₃₃N₃O₆S

Base Information

Chemical Name:C₂₄H₃₃N₃O₆S
CAS No.:1290128-16-3
Molecular Formula:C₂₄H₃₃N₃O₆S
Molecular Weight:491.609
Hs Code.:

C<sub>24</sub>H<sub>33</sub>N<sub>3</sub>O<sub>6</sub>S

Synonyms:C₂₄H₃₃N₃O₆S

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Chemical Property of C₂₄H₃₃N₃O₆S

Chemical Property:

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Technology Process of C₂₄H₃₃N₃O₆S

There total 9 articles about C₂₄H₃₃N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₇N₃O₆S

: 107-08-4
1-iodo-propane

: 1290128-16-3
C₂₄H₃₃N₃O₆S

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.333333h;

Reference yield:

: 1190854-60-4
ethyl 6-oxo-5,6-dihydropyrazolo[5,1-b][1,3]thiazole-7-carboxylate

: 1290128-16-3
C₂₄H₃₃N₃O₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

2.1: sodium hydroxide; water / ethanol / 2 h / 20 - 80 °C

2.2: Cooling with ice

2.3: 1.5 h / 60 °C

3.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 20 °C / Cooling with ice

3.2: Cooling with ice

3.3: 5 h / 20 °C / 760.05 Torr

4.1: triethylamine / dichloromethane / 11 h / 20 °C

5.1: n-butyllithium / hexane; tetrahydrofuran / 0.67 h / -78 °C

5.2: 2 h

6.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water / 2.58 h / 110 °C / Reflux

7.1: potassium carbonate / N,N-dimethyl-formamide / 16.17 h / 20 °C

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

With hydrogenchloride; n-butyllithium; water; sodium hydride; potassium carbonate; caesium carbonate; triethylamine; sodium hydroxide; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1190854-64-8
6-methoxypyrazolo[5,1-b]thiazole-7-carboxylic acid

: 1290128-16-3
C₂₄H₃₃N₃O₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; diphenyl phosphoryl azide / 1,4-dioxane / 3 h / 20 °C / Reflux

1.2: 3 h / 20 °C / Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.67 h / -78 °C

2.2: 2 h

3.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water / 2.58 h / 110 °C / Reflux

4.1: potassium carbonate / N,N-dimethyl-formamide / 16.17 h / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

With n-butyllithium; diphenyl phosphoryl azide; sodium hydride; potassium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; hexane; water; N,N-dimethyl-formamide; mineral oil;