3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

Base Information

Chemical Name:3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione
CAS No.:1293965-65-7
Molecular Formula:C₂₃H₂₅NO₂S₂
Molecular Weight:411.589
Hs Code.:

Synonyms:3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

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Chemical Property of 3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

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Technology Process of 3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

There total 2 articles about 3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₃₀N₂O

: 529477-58-5
N-(hydroxy)-5-(p-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 1293965-65-7
3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 1293965-62-4
2-((1-methyl-1-phenylpent-4-en-2-yl)sulfanyl)-5-(4-methoxyphenyl)-4-methylthiazole N-oxide

Guidance literature:: In dichloromethane; at -30 ℃;
DOI:10.1016/j.tet.2010.12.071

Reference yield:

: 85924-68-1
2-phenylhex-5-en-2-ol

: 1293965-65-7
3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 1293965-62-4
2-((1-methyl-1-phenylpent-4-en-2-yl)sulfanyl)-5-(4-methoxyphenyl)-4-methylthiazole N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride / 20 °C

2: dichloromethane / -30 °C

With copper(l) chloride; In dichloromethane;
DOI:10.1016/j.tet.2010.12.071

Reference yield: 45.0%

: 75-62-7
Bromotrichloromethane

: 1293965-65-7
3-(1-methyl-1-phenylpent-4-en-1-oxy)-5-(4-methoxyphenyl)-4-methylthiazole-2(3H)-thione

: 902757-52-2
1,2-bis[5-(4-methoxyphenyl)-4-methylthiazol-2-yl]disulfane

: trans-5-bromomethyl-2-methyl-2-phenyltetrahydrofuran

: 2-(bromomethyl)-5-(phenyl)-5-(methyl)tetrahydrofuran

: 85924-68-1
2-phenylhex-5-en-2-ol

: 4-methyl-5-(4-methoxyphenyl)-2-(trichloromethylsulfanyl)thiazole-2(3H)-thione

Guidance literature:: In benzene; at 25 ℃; for 0.583333h; optical yield given as %de; diastereoselective reaction; Photolysis;
DOI:10.1016/j.tet.2010.12.071