4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

Base Information

Chemical Name:4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide
CAS No.:129967-40-4
Molecular Formula:C₂₅H₂₇NO₃
Molecular Weight:389.494
Hs Code.:

Synonyms:4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

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Chemical Property of 4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

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Technology Process of 4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

There total 4 articles about 4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 129967-39-1
3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid

: 104-94-9
4-methoxy-aniline

: 129967-40-4
4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In dichloromethane; for 12h;
DOI:10.1021/jo00310a019

Reference yield:

: 40614-20-8
3-(2'-Hydroxyphenyl)-3,3-dimethylpropanol

: 129967-40-4
4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / K₂CO₃, KI / acetone / 12 h / Heating

2: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h

3: 72 percent / AgNO₃, aq. KOH / ethanol / 2.5 h

4: 44 percent / dicyclohexylcarbodiimide / 4-(dimethylamino)pyridine / CH₂Cl₂ / 12 h

With potassium hydroxide; potassium carbonate; silver nitrate; dicyclohexyl-carbodiimide; pyridinium chlorochromate; potassium iodide; dmap; In ethanol; dichloromethane; acetone;
DOI:10.1021/jo00310a019

Reference yield:

: 129967-38-0
3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionaldehyde

: 129967-40-4
4-Methoxyaniline 3-(2'-(Benzyloxy)phenyl)-3,3-dimethylpropionic Acid Amide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / AgNO₃, aq. KOH / ethanol / 2.5 h

2: 44 percent / dicyclohexylcarbodiimide / 4-(dimethylamino)pyridine / CH₂Cl₂ / 12 h

With potassium hydroxide; silver nitrate; dicyclohexyl-carbodiimide; dmap; In ethanol; dichloromethane;
DOI:10.1021/jo00310a019