Technology Process of C49H45NO9
There total 5 articles about C49H45NO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
tetrahydrofuran; water; toluene;
at 80 ℃;
for 24.25h;
Inert atmosphere;
DOI:10.1002/ejoc.201200484
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / acetonitrile / 0.25 h
1.2: 24 h / 75 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water; toluene / 24.25 h / 80 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate; potassium carbonate;
In
tetrahydrofuran; water; toluene; acetonitrile;
2.1: Suzuki coupling;
DOI:10.1002/ejoc.201200484
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / diethyl ether / Reflux
2.1: sulfuric acid; hydrogen bromide / water / Reflux
3.1: potassium carbonate / acetonitrile / 0.25 h
3.2: 24 h / 75 °C / Inert atmosphere
4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water; toluene / 24.25 h / 80 °C / Inert atmosphere
With
lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); sulfuric acid; hydrogen bromide; sodium carbonate; potassium carbonate;
In
tetrahydrofuran; diethyl ether; water; toluene; acetonitrile;
4.1: Suzuki coupling;
DOI:10.1002/ejoc.201200484
