2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

Base Information

Chemical Name:2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose
CAS No.:849501-74-2
Molecular Formula:C₅₆H₄₉NO₁₇
Molecular Weight:1008
Hs Code.:

Synonyms:2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

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Chemical Property of 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

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Technology Process of 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

There total 11 articles about 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.8%

: 849501-67-3
p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

: 849501-74-2
2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; at 20 ℃; for 20h;
DOI:10.3987/COM-04-S(P)28

Reference yield:

: 97589-70-3
3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

: 849501-74-2
2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 92.4 percent / pyridine / 20 h / 20 °C

2: 86.1 percent / N-bromosuccinimide / CCl₄ / 0.5 h / Irradiation

3: 78.8 percent / cerium ammonium nitrate / acetonitrile; H₂O / 20 h / 20 °C

With N-Bromosuccinimide; ammonium cerium(IV) nitrate; In pyridine; tetrachloromethane; water; acetonitrile;
DOI:10.3987/COM-04-S(P)28

Reference yield:

: 97523-39-2
3,6-di-O-benzoyl-2-(benzoyloximino)-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-arabino-hexopyranosyl bromide

: 849501-74-2
2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 78.8 percent / cerium ammonium nitrate / acetonitrile; H₂O / 20 h / 20 °C

With ammonium cerium(IV) nitrate; In water; acetonitrile;
DOI:10.3987/COM-04-S(P)28