p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside
• CAS No.: 849501-67-3
• Molecular Formula: C₆₄H₅₇NO₁₈
• Molecular Weight: 1128.15

Synonyms:p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

Chemical Property of p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

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Technology Process of p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

There total 12 articles about p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.1%

acetic anhydride (108-24-7) + 3,6-di-O-benzoyl-2-(benzoyloximino)-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-arabino-hexopyranosyl bromide (97523-39-2) + 4-Methoxybenzyl alcohol (105-13-5) → C57H53NO17 + p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside (849501-67-3) + C64H57NO18

Guidance literature:

Multistep reaction;

DOI:10.3987/COM-04-S(P)28

Reference yield: 46.0%

acetic anhydride (108-24-7) + 4-Methoxybenzyl alcohol (105-13-5) + 3,6-di-O-benzoyl-2-(p-chlorobenzoyloxyimino)-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-arabino-hexopyranosyl bromide → C57H53NO17 + p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside (849501-67-3) + C64H57NO18

Guidance literature:

Multistep reaction;

DOI:10.3987/COM-04-S(P)28

Reference yield: 44.6%

acetic anhydride (108-24-7) + 4-Methoxybenzyl alcohol (105-13-5) + 3,6-di-O-benzoyl-2-(p-methylbenzoyloxyimino)-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-arabino-hexopyranosyl bromide → C57H53NO17 + p-Methoxybenzyl 2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside (849501-67-3) + C64H57NO18

Guidance literature:

Multistep reaction;

DOI:10.3987/COM-04-S(P)28

upstream raw materials:

acetic anhydride

3,6-di-O-benzoyl-2-(benzoyloximino)-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-α-D-arabino-hexopyranosyl bromide

4-Methoxybenzyl alcohol

3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1,5-anhydro-D-fructose oxime

Downstream raw materials:

2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranosyl chloride

2-acetamido-3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranose

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