N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

Base Information

Chemical Name:N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide
CAS No.:330983-57-8
Molecular Formula:C₂₃H₂₃ClN₂O₆
Molecular Weight:458.898
Hs Code.:

Synonyms:N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

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Technology Process of N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

There total 1 articles about N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 931-53-3
Cyclohexyl isocyanide

: 3740-52-1
2-(2-nitrophenyl)acetic acid

: 4998-15-6
4-chlorophenylglyoxal

: 330983-57-8
N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

Guidance literature:: In diethyl ether; at 20 ℃; for 24h;
DOI:10.1002/jhet.5570370615

Reference yield: 76.0%

: 330983-57-8
N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

: 330983-61-4
N-cyclohexyl 3-(4-chlorophenyl)-2,5-dihydro-2-(2-nitrophenyl)-5-oxofuran-2-carboxamide

Guidance literature:: N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide; With piperidine; In ethanol; at 20 ℃; for 0.166667h;

With hydrogenchloride; In ethanol; pH=4;
DOI:10.1002/jhet.5570370615

Reference yield:

: 330983-57-8
N-cyclohexyl 3-(4-chlorophenyl)-2-(2-nitrophenyl)acetoxy-3-oxopropionamide

: N-cyclohexyl (Z)-3-(4-chlorophenyl)-3-(2,3-dihydro-2-oxoindol-3-ylidene)-2-hydroxypropionamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperidine / ethanol / 0.17 h / 20 °C

1.2: 76 percent / 6N aq. HCl / ethanol / pH 4

2.1: 91 percent / Fe; AcOH / 0.25 h / 60 - 65 °C

With piperidine; iron; acetic acid; In ethanol; 1.1: Knoevenagel condensation;
DOI:10.1002/jhet.5570370615