C₄₈H₅₅N₇O₁₁S₂Si

Base Information

Chemical Name:C₄₈H₅₅N₇O₁₁S₂Si
CAS No.:175916-18-4
Molecular Formula:C₄₈H₅₅N₇O₁₁S₂Si
Molecular Weight:998.223
Hs Code.:

C<sub>48</sub>H<sub>55</sub>N<sub>7</sub>O<sub>11</sub>S<sub>2</sub>Si

Synonyms:C₄₈H₅₅N₇O₁₁S₂Si

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Chemical Property of C₄₈H₅₅N₇O₁₁S₂Si

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Technology Process of C₄₈H₅₅N₇O₁₁S₂Si

There total 3 articles about C₄₈H₅₅N₇O₁₁S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 507-09-5
tiolacetic acid

: 175916-15-1
C₄₅H₅₃N₅O₁₂SSi

: 175916-18-4
C₄₈H₅₅N₇O₁₁S₂Si

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; acetonitrile; for 0.75h; Ambient temperature;
DOI:10.1021/ja952322m

Reference yield:

: 175916-09-3
C₆₁H₆₃N₅O₁₃SSi

: 175916-18-4
C₄₈H₅₅N₇O₁₁S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: oxone, aq. NaOAc / methanol; tetrahydrofuran / Ambient temperature

2: 54 percent / 0.2 M aq. LiOH / methanol; tetrahydrofuran / 1.5 h / 0 °C

3: 92 percent / PPh₃, DIAD / acetonitrile; tetrahydrofuran / 0.75 h / Ambient temperature

With Oxone; lithium hydroxide; di-isopropyl azodicarboxylate; sodium acetate; triphenylphosphine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja952322m

Reference yield:

: 175916-19-5
C₆₁H₆₃N₅O₁₅SSi

: 175916-18-4
C₄₈H₅₅N₇O₁₁S₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / 0.2 M aq. LiOH / methanol; tetrahydrofuran / 1.5 h / 0 °C

2: 92 percent / PPh₃, DIAD / acetonitrile; tetrahydrofuran / 0.75 h / Ambient temperature

With lithium hydroxide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja952322m