N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

Base Information

Chemical Name:N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide
CAS No.:628300-71-0
Molecular Formula:C₂₁H₁₉ClN₂O₅S
Molecular Weight:446.911
Hs Code.:

Synonyms:N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

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Chemical Property of N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

Chemical Property:

Boiling Point:696.8±65.0 °C(Predicted)
Density:1.35±0.1 g/cm3(Predicted)

Purity/Quality:

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Technology Process of N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

There total 7 articles about N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: N-[4-chloro-2-(pyridine-4-carbonyl)phenyl]-4-isopropoxybenzenesulfonamide

: 628300-71-0
N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 106-47-8
4-chloro-aniline

: 628300-71-0
N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trichloride / Trichloroethylene; dichloromethane / 0.17 h / 0 °C

1.2: 14.5 h / 20 - 85 °C

1.3: 1.5 h / 20 - 115 °C

2.1: pyridine / 70 - 80 °C

2.2: 5.5 h / 70 - 80 °C

3.1: acetic acid; dihydrogen peroxide / water / 8 h / 50 - 60 °C

With pyridine; dihydrogen peroxide; boron trichloride; acetic acid; In dichloromethane; Trichloroethylene; water;

Reference yield:

: 52482-36-7
morpholin-4-yl(pyridin-4-yl)methanone

: 628300-71-0
N-{4-chloro-2-[(1-oxidopyridin-4-yl)carbonyl]phenyl}-4-(propan-2-yloxy)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -30 - -20 °C / Inert atmosphere

1.2: 4 h / 15 - 25 °C / Inert atmosphere

1.3: 4 h / 55 - 65 °C

2.1: pyridine / 70 - 80 °C

2.2: 5.5 h / 70 - 80 °C

3.1: acetic acid; dihydrogen peroxide / water / 8 h / 50 - 60 °C

With pyridine; n-butyllithium; dihydrogen peroxide; acetic acid; In tetrahydrofuran; hexane; water;