triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

Base Information

Chemical Name:triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate
CAS No.:1190383-75-5
Molecular Formula:C₂₃H₂₉NO₆
Molecular Weight:415.486
Hs Code.:

Synonyms:triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

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Chemical Property of triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

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Technology Process of triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

There total 5 articles about triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 141-97-9
ethyl acetoacetate

: 121641-60-9
ethyl 2-(4-methylphenylimino)acetate

: 1190383-75-5
triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

Guidance literature:: With copper(ll) bromide; at 20 ℃; for 18h; Neat (no solvent);
DOI:10.2174/157017809787893082

Reference yield: 87.0%

: 1190383-94-8
diethyl 2-acetyl-3-(p-tolylamino)succinate

: 141-97-9
ethyl acetoacetate

: 1190383-75-5
triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

Guidance literature:: With tris[2-phenylpyridinato-C₂,N]iridium(III); bis(1-methyl-1-phenylethyl)peroxide; In toluene; at 20 ℃; for 5h; Irradiation;
DOI:10.1016/j.tet.2020.131353

Reference yield: 86.0%

: 924-44-7
glyoxylic acid ethyl ester

: 141-97-9
ethyl acetoacetate

: 106-49-0,12221-03-3
p-toluidine

: 1190383-75-5
triethyl 2,6-dimethyl-1-(p-tolyl)-1,4-dihydropyridine-3,4,5-tricarboxylate

Guidance literature:: With montmorillonite K-10; at 20 ℃; for 12h; Reagent/catalyst; Concentration; Green chemistry;
DOI:10.1016/j.tet.2013.04.006