C₆₂H₆₀N₈Ni

Base Information

Chemical Name:C₆₂H₆₀N₈Ni
CAS No.:1309146-34-6
Molecular Formula:C₆₂H₆₀N₈Ni
Molecular Weight:975.902
Hs Code.:

C<sub>62</sub>H<sub>60</sub>N<sub>8</sub>Ni

Synonyms:C₆₂H₆₀N₈Ni

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Chemical Property of C₆₂H₆₀N₈Ni

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Technology Process of C₆₂H₆₀N₈Ni

There total 2 articles about C₆₂H₆₀N₈Ni which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₁H₆₂N₈Ni

: 149-73-5
trimethyl orthoformate

: 1309146-34-6
C₆₂H₆₀N₈Ni

Guidance literature:: C₆₁H₆₂N₈Ni; trimethyl orthoformate; With hydrogenchloride; In water; toluene; at 90 ℃; for 1h; Inert atmosphere;

With potassium carbonate; In chloroform; water; toluene;
DOI:10.1021/ol2010215

Reference yield:

: 944133-08-8
(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiCHN₂H

: 1309146-34-6
C₆₂H₆₀N₈Ni

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium nitrate; acetic anhydride; acetic acid / chloroform / 3 h / 45 °C

1.2: 1 h / Reflux

2.1: sodium tetrahydroborate; palladium 10% on activated carbon / methanol; dichloromethane / 1 h / 25 °C / Inert atmosphere

3.1: hydrogenchloride / water; toluene / 1 h / 90 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; palladium 10% on activated carbon; lithium nitrate; acetic anhydride; acetic acid; In methanol; dichloromethane; chloroform; water; toluene;
DOI:10.1021/ol2010215

Reference yield: 95.0%

: 1309146-34-6
C₆₂H₆₀N₈Ni

: 74-88-4
methyl iodide

: C₆₆H₇₀N₈Ni⁽²⁺⁾*2I^(1-)

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere; Schlenk technique;
DOI:10.1142/S1088424619501128 DOI:10.1039/d0dt00594k