<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

Base Information

Chemical Name:<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane
CAS No.:129986-07-8
Molecular Formula:C₃₅H₅₉Cl₃O₇Si
Molecular Weight:726.294
Hs Code.:

<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

Synonyms:<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

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Chemical Property of <1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

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Technology Process of <1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

There total 4 articles about <1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 84439-58-7
(2,2,2-trichloroethoxy)methyl bromide

: 129986-06-7,130061-19-7
<2S,3R,4R,6R,8S,8(2R),9S>-3,9-dimethyl-8-<2-<<(1-methylethyl)diethylsilyl>oxy>butyl>-2-<2-<(4-methoxyphenyl)methoxy>ethyl>-1,7-dioxaspiro<5.5>undecan-4-ol

: 129986-07-8
<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

Guidance literature:: With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In acetonitrile; for 18.5h; Ambient temperature;
DOI:10.1021/ja00175a038

Reference yield:

: 107149-56-4
chlorodiethylisopropylsilane

: 129986-07-8
<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / imidazole / CH₂Cl₂ / 2.6 h / Ambient temperature

2: 98 percent / SmI₂/i-PrOH / tetrahydrofuran / 3 h / 23 °C

3: 97 percent / 1,8-bis(dimethylamino)naphthalene / acetonitrile / 18.5 h / Ambient temperature

With 1H-imidazole; samarium diiodide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; isopropyl alcohol; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ja00175a038

Reference yield:

: 129986-04-5
<2S,3R,6R,8S,8(2R),9S>-3,9-dimethyl-8-(2-hydroxybutyl)-2-<2-<(4-methoxyphenyl)methoxy>ethyl>-1,7-dioxaspiro<5.5>undecan-4-one

: 129986-07-8
<1(2S,3R,4S,6R,8S,9S),2R>-<1-<3,9-dimethyl-2-<<(4-methoxyphenyl)methoxy>ethyl>-4-<(2,2,2-trichloroethoxy)methoxy>-1,7-dioxaspiro<5.5>undecan-8-yl>-2-butoxy>(1-methylethyl)diethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / imidazole / CH₂Cl₂ / 2.6 h / Ambient temperature

2: 98 percent / SmI₂/i-PrOH / tetrahydrofuran / 3 h / 23 °C

3: 97 percent / 1,8-bis(dimethylamino)naphthalene / acetonitrile / 18.5 h / Ambient temperature

With 1H-imidazole; samarium diiodide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; isopropyl alcohol; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ja00175a038