2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

Base Information

Chemical Name:2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester
CAS No.:189340-39-4
Molecular Formula:C₂₁H₂₆ClNO₆S
Molecular Weight:455.96
Hs Code.:

Synonyms:2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

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Chemical Property of 2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

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Technology Process of 2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

There total 2 articles about 2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 189339-69-3
2-chlorobenzenesulfonic acid 3-hydroxy-5-methylphenyl ester

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 189340-39-4
2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

Guidance literature:: In tetrahydrofuran; water;

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 189339-69-3
2-chlorobenzenesulfonic acid 3-hydroxy-5-methylphenyl ester

: 189340-39-4
2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 25 ℃;
DOI:10.1016/S0960-894X(98)00290-X

Reference yield:

: 189340-39-4
2-Chlorobenzenesulfonic acid 3-[[3-N-(tert-butoxycarbonyl)amino]propoxy]-5-methylphenyl ester

: 2-Chloro-benzenesulfonic acid 3-(3-guanidino-propoxy)-5-methyl-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / dioxane

2: DIEA / dimethylformamide

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(98)00290-X