Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester

Base Information

• Chemical Name: Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester
• CAS No.: 104966-92-9
• Molecular Formula: C₂₁H₃₂O₆
• Molecular Weight: 380.481

Synonyms:Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester

Chemical Property of Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester

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Technology Process of Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester

There total 8 articles about Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

10-acetoxydecanoyl chloride (104967-12-6) + 3,4,5-trimethoxytoluene (6443-69-2) → 6-(10-acetoxy-1-oxodecyl)-2-hydroxy-3-methoxy-5-methylphenol (104967-09-1) + Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester (104966-92-9)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at 20 ℃; for 72h;

DOI:10.1248/cpb.33.4422

Reference yield: 44.0%

10-acetoxydecanoyl chloride (104967-12-6) + 3,4,5-trimethoxytoluene (6443-69-2) → 6-(10-acetoxy-1-oxodecyl)-2-hydroxy-3-methoxy-5-methylphenol (104967-09-1) + 6-(10-acetoxy-1-oxodecyl)-3-hydroxy-2-methoxy-5-methylphenol (104967-08-0) + Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester (104966-92-9)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at 20 ℃; for 72h;

DOI:10.1248/cpb.33.4422

Reference yield: 29.0%

10-acetoxydecanoyl chloride (104967-12-6) + 3,4,5-trimethoxytoluene (6443-69-2) → Acetic acid 10-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-10-oxo-decyl ester (104966-92-9) + 2-(10-acetoxy-1-oxodecyl)-3,4,5-trimethoxytoluene (104967-07-9)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at 20 ℃; for 72h;

DOI:10.1248/cpb.33.4422

upstream raw materials:

10-acetoxydecanoyl chloride

3,4,5-trimethoxytoluene

9-bromononan-1-ol

9-bromononyl acetate

Downstream raw materials:

6-(10-hydroxydecyl)-2,3-dimethoxy-5-methylphenol

6-(10-acetoxydecyl)-2,3-dimethoxy-5-methylphenol

2,3-dimethoxy-5-methyl-6-(10'-acetoxydecyl)-1,4-benzoquinone

Idebenone

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