dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

Base Information

Chemical Name:dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester
CAS No.:909724-13-6
Molecular Formula:C₁₄H₁₈O₅S₂
Molecular Weight:330.426
Hs Code.:

Synonyms:dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

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Chemical Property of dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

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Technology Process of dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

There total 2 articles about dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 51490-01-8
1-(3,4,5-trimethoxyphenyl)-2-bromoethanone

: 140-89-6
potassium ethyl xanthogenate

: 909724-13-6
dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

Guidance literature:: In acetone; at 20 ℃; for 1h;
DOI:10.1021/jm060804a

Reference yield: 63.0%

: 7702-09-2
2-diazo-1-(3,4,5-trimethoxyphenyl)ethanone

: 140-89-6
potassium ethyl xanthogenate

: 909724-13-6
dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

Guidance literature:: 2-diazo-1-(3,4,5-trimethoxyphenyl)ethanone; With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃;

potassium ethyl xanthogenate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1055/a-1513-9968

Reference yield: 69.0%

: 909724-13-6
dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester

: 165334-43-0
(Z)-3-chloro-3-(2-methoxyphenyl)acrylaldehyde

: 1036271-21-2
C₂₁H₂₀O₅S

Guidance literature:: dithiocarbonic acid O-ethyl ester S-[2-oxo-2-(3,4,5-trimethoxyphenyl)-ethyl] ester; With piperidine; In ethanol; at 20 ℃; for 0.5h;

(Z)-3-chloro-3-(2-methoxyphenyl)acrylaldehyde; In ethanol; for 3h; Further stages.; Heating;
DOI:10.1016/j.bmc.2008.04.026